SEM PHOTOS

McKittrick Wells
Ruth Kramer, MTU, Analyst

Electron images are either secondary electron images (SEIs) or Backscattered electron images (BEIs). SEIs are created from low energy electrons which escape from the surface of the specimen. They give detailed morphological information; our JEOL JSM 820 can produce excellent images at 50,000X, and has a maximum resolution of 20 nm. BEIs are produced as impinging electrons are scattered back by the specimen. Light elements (carbon, etc) are less capable of backscattering. Iron and heavier elements are more capable of backscattering. Therefore, heavy elements appear bright, and lighter elements appear dark. Backscattering occurs from deeper in the specimen, and from a larger volume. Therefore, BEIs have at least an order of magnitude poorer resolution than SEIs. However, for most of our applications, backscatter resolution is more than adequate. In these specimens, pyrite is usually bright framboids and easy to recognize. Feldspars are often lath to squarish and frequently show disequilibrium as in photo 1638. Silica occurs as detrital quartz grains, microfossils, and mostly as amorphous cement. Calcite is not common except in carbonate hard streak or as fossils. Gypsum and sphene are fine grained minor accessory phases.

Photo
#
Well and Depth Magnification/Type/Description
1430 418-1430.5 250X BEI concentrations of heavy elements appear bright and lighter elements appear dark. Shows pyritized (bright) microfossil tests in a matrix of silica (dark gray), patches of hydrocarbon (black), and tiny curved calcareous test (bright gray). Pyrite framboids appear as 5m white circles in the matrix.
1636 418-1631.5 V 500X BEI shows hydrocarbon (black), silica, feldspars, pyrite
1637 418-1631.5V 500X SEI shows hydrocarbon, silica, feldspars, pyrite. Same field as 1636. There appears to be a textural difference between the silica immediately surrounding the hydrocarbon, and the open porosity (recognized by the charging edges of the open pores).
1638 418-1631.5V 750X BEI showing alteration (?) of feldspar; sodic patches (dark) and potassic (brighter).
1639 418-1631.5V 250X BEI This seems to show a silica fossil whose pores are filled with hydrocarbon.
1640 418-1631.5V 750X BEI which is a higher magnification than the previous, showing a diatom fossil filled with hydrocarbon.
1641 418-1631.5 l000X BEI pyritized shell-gypsum in chamber. The lathlike pieces at the bottom are calcium carbonate. Large detrital (?) grains are plagioclase and ksp
1723 418 1723.7A 250X BEI/ fractures, etc. "clay rich". Note that calcite rhombs in alteration region are more abundant than in majority portion of section. Fractures are filled with blue epoxy.
1724 418 1723.7A 1000X BEI of alteration region along fracture. The 10 semi-quantitative point analyses indicated that there are small quantities of Al(2)0(3) with the silica phase. Sphene, pyrite, and feldspar (anorthoclase) were found.
1754 418 1754.5A 250X BEI/ fine grained "cherty" sample. Pyrite, calcite, and other detrital phases constitute approximately 1-2% of the rock.
1755 418 1754.5A 1000X BEI. The groundmass analyzes as mostly silica, with contamination by fine grained authigenic phases (framboidal pyrite, calcite). Detrital albite is the large grain. Note: vey fine porosity; unpenetrated by epoxy.

(Filename:Thinsections)
Last Update: 1/16/95

The first set of samples selected for petrographic analysis were the following (H = horizontal and V = vertical):

Sample Description/reason Optical
Petrographic
Description?
SEM Slide Done? Optical Slide Done?
1145.7 Opal A-Vertical Fx Yes No No
1186.5 Opal A-No tendency to vertical fx Yes No Yes
1753.5 Opal CT- non-fracturing Yes No No
1757.5 Opal CT-Fractured Yes No No
1228.8 Opal A-Low clay, High So Yes No No-V and H
1230.4 Opal A-High clay, Low So Yes No No-B
1401.5 Carbonate Hard Streak Yes No No-V
1526.7 Sample w/ carbonate cement above and below Yes Yes No-V and H
1465.5 Opal A/CT transition: Low clay, A rich Yes No No
1522.6 Opal A/CT transition: 50:50 Yes No Yes-V
1631.5 Opal A/CT transition: High Clay, CT rich Yes Yes Yes-V and H
1754.5 Siltstones Yes Yes Yes-V
1681.5 Opal CT-low clay Yes No No-H
1723.7 Opal CT-high clay Yes Yes Yes-V and H
1753.5 Cherty, downsection Yes No No-V and H
1622 Opal A/CT Transition w/ So=0 No No No

The samples were sent for polished thin sections and two sections were requested for each sample--one cut parallel to the bedding (H) and one cut perpendicular to the bedding (V).

SELECTED LATER
Sample Description/reason Optical
Petrographic
Description?
SEM Slide Done? Optical Slide Done?
1660 Yes No No
1572.4 Yes Yes Yes-V and H
1424.5 Yes No No
1399.5 Yes No No
1573.5 Yes No Yes-V
1756.5 Yes No Yes-V
1757.5 Yes No No-V and H
1634.8 Yes -V and H
1431.5 Yes -V and H